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Barite Plugs Applications, Formulation & Operation

Introduction To Barite Plugs

Barite plug use is normally limited to extreme or emergency conditions where it is imperative that some measures be taken to seal off the bottom section of the wellbore. This type of plug is applicable in several situations including:

  • Simultaneous kicking and lost circulation.
  • Well Abandonment procedure allows the safe withdrawal of drill pipe to allow setting of cement plug.
  • Withdrawal of drill pipe to either set casing or repair existing casing strings.
  • Plugging drill pipes in emergency situations.
  • High-pressure salt water flows where required kill mud weight approaches or exceeds the formation breakdown equivalent at some point in the open hole, usually the last casing shoe.

Objectives of Setting Barite Plugs

A Barite plug is basically a slurry of barite that is pumped down the drill pipe and placed at the bottom of the wellbore. A successful Barite plug should accomplish two things:

  1. Initially, the weight of the barite slurry should kill the well.
  2. After a period of time, the settled barite plug should mechanically block any flow up the wellbore.

The well should be killed before a mechanical blockage is established in the wellbore.

Barite Plug Design

Designing a barite plug for killing a well or curing circulation loss is straightforward. The barite slurry pumped into the well must be heavy enough and fill enough of the wellbore to increase the bottom hole pressure to a level exceeding the formation pressure. Problems arise when formation pressure is unknown or when the weight or volume of the required barite slurry becomes excessive.

Designing a barite plug to physically block the wellbore is somewhat more complicated. The generally accepted method is to mix a slurry so that the barite settles out from the slurry into a hard plug which will block the wellbore. The rate that barite will settle into a hard plug is usually slow and predictable. Fairly accurate field predictions may be made from an observation of the initial barite settling rate in a small container. The initial rate is constant and independent of the height of the slurry. The initial settling rate lasts for a short period of time, after which the settling rate decreases as fewer barite particles remain in suspension. In a container one foot high, the initial settling rate applies for approximately five minutes. In a field situation with 500 or more feet (150 or more meters) of barite slurry, the initial rate may apply for a day or longer. The amount of barite settling in a shorter period can be computed as the product of the initial rate times the waiting time.

Field experience has shown that slurries of up to 20 lbs/gal (2.40 SG) are relatively easily prepared using only Base Oil, EZ MUL (Oil Wetting Agent), DRILTREAT, and Barite for oil muds. Water, SAPP, caustic soda, and barite are used for Water Based Mud.

Barite Plug Preparation

From a practical point of view, the following points should be considered:
Use of a cement unit is preferable. This requires that either bulk barite be fed directly to the cement unit surge tank or that sufficient stocks of sacked barite be available at the rig site.

Standard plugs can be mixed to the desired density with no problems of massive settling before
displacement.

Oil Based Mud

Oil Mud Application

Barite plug settling rates in oil muds are normally dependent on the density of the slurry and the type and concentration of oil wetting agents. Laboratory studies have shown that oil-based plugs have a tendency to settle, on average, more slowly than water-based slurries.

At too low a concentration of EZ MUL and DRILTREAT the barite is insufficiently oil-wet and is not self-suspending. At too high a concentration the barite becomes extremely well suspended and the rate of settling is reduced. It is therefore very important to carefully select the optimum concentration of EZ MUL for the plug density required.

If a cement unit is not able to mix barite, use a slug pit or the reserve mud pits, depending on the total volume of slurry required. The length of the plug is a wellsite determination and should be based on the severity of the situation. In most cases a plug in the range of 250 – 500 ft (75-150 m) is sufficient.

Oil-Based Mud Procedure

Oil-based mud slurries can be mixed as follows:

  1. Transfer sufficient Oil Based Mud to the slug pit to maintain circulation through the mixing pump.
  2. Fill the pit to half its capacity with a base oil and add approximately 4 lbs/bbl (11.4 kg/m3) EZ MUL and 4 lbs/bbl (11.4 kg/m3) DRILTREAT.
  3. Weight up with barite to the required density; the pit should then be nearly full.
  4. If the total capacity of the slug pit is insufficient for the required volume of the plug, transfer the slurry already mixed to a reserve pit making sure that agitators are used constantly and another mixing pump put on to circulate that pit.

The Mud Engineer on site should ensure that the following measures are also adhered to:

  • To avoid the chance of initiating rapid settling, excessive additions of base oil are not made at any stage.
  • Small additions of up to 1.5 lbs/gal (4.3 kg/m3) EZ MUL may be made to control viscosity increases noted during barite additions.
  • Barite addition rate is controlled in order to avoid excessive increases in viscosity or possibly initiating settling.

Formulations for oil-base muds:

oil base mud barite plug

Water Based Mud

Water-Based Mud Application

The slurry is composed of barite, fresh water, sodium acid pyrophosphate (SAPP) and caustic soda. SAPP, a thinner, increases the barite settling rate by lowering the yield point (check also Yield Point In Drilling Mud Formula) and gel strength of the slurry, and the caustic soda is added to provide an alkaline environment (pH = 10).

The formulation for one barrel of a 20 lbs/gal barite slurry is:

water base mud barite plug

OR

formulation

Displacement

Displacement techniques are the same as in cementing; i.e., the slurry should be under-displaced so that the height of the slurry in the drill pipe is 2 bbls greater than in the annulus. This allows the drill pipe to be withdrawn with a natural slugging action. It will also minimize the movement of the slurry in the hole, reducing contamination.

Because of the high density of these slurries, high differential pressures can be created by under or over-displacement. Care must be taken when calculating volumes. After the plug is spotted in place, tripping out of the hole should be done as quickly as possible and the plug allowed to settle for several hours. The well should be observed to ensure there is no flow. When tripping pipe back into the hole, the “feeling” for the plug should begin near the theoretical top of the plug.

Operations can then be started to set a cement plug above the barite, and the well can be safely secured.

Barite Plug Papers

https://www.semanticscholar.org/paper/Potential-of-Barite-Weighted-Epoxy-Systems-to-Plug-Gao/6e956f2e53d8a0c2f83eea11a2f9087420a4e82a